Methanesulfonyl chloride → HCID 22567201, 화합물

HRID 25392

반응식

HRID 25392 반응식
[NH2:1][C:2]1[C:10]2[C:5](=[CH:6][CH:7]=[C:8]([N+:11]([O-:13])=[O:12])[CH:9]=2)[NH:4][N:3]=1.[CH3:14][S:15](Cl)(=[O:17])=[O:16]>N1C=CC=CC=1>[CH3:14][S:15]([NH:1][C:2]1[C:10]2[C:5](=[CH:6][CH:7]=[C:8]([N+:11]([O-:13])=[O:12])[CH:9]=2)[NH:4][N:3]=1)(=[O:17])=[O:16]

참가 물질

4

반응물 2

HCID 31297Methanesulfonyl chlorideHCID 31366553-Amino-5-nitroindazole

생성물 1

HCID 22567201HCID 22567201, 화합물수율 84.4%

시약·촉매·용매 1

HCID 1049Pyridine용매

실험 절차

3-Methylsulfonylamino-5-nitro-1H-indazole can be obtained as described in Example 2 from 0.7 g of 3-amino-5-nitro-1H-indazole, 23 ml of pyridine and 0.455 g of methylsulfonyl chloride. 0.85 g of 3-methylsulfonylamino-5-nitro-1H-indazole is thus obtained in the form of an orange powder used as it is in the following step.

출처 및 근거

ORD 기록
ord-326bba7b2f4f49ab91dc51bf762c3c23
출처 데이터셋
uspto-grants-2005_02
특허 번호
US06858638B2

연결된 노트

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