Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → N-(4-Fluoro-2-(4-methyl-1H-imidazol-1-yl)phenyl)acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 4-Fluoro-2-(4-methyl-1H-imidazol-1-yl)aniline | HCID 57732445 | — |
| 생성물 | N-(4-Fluoro-2-(4-methyl-1H-imidazol-1-yl)phenyl)acetamide | HCID 57732446 | 64% |
반응 단계
Reaction of intermediate 2A (17.5 g, 91.4 mmol) and acetic anhydride (90 mL, 914 mmol) provided the product 3A as an off-white powder (13.5 g, 64% yield). EIMS 234.1 [M+H]+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07875618B2 |
| 출처 데이터셋 | uspto-grants-2011_01 |
| ORD ID | ord-49d3eb530c804cd2bbf6799cdfdc0461 |
| 출처 메모 | uspto-grants-2011_01 |