Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzoic acid, 3-isothiocyanato- → 3-{3-[5-(5,6-Dichloro-1H-indol-2-yl)-2-methoxy-phenyl]-thioureido}-benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzoic acid, 3-isothiocyanato- | HCID 75046 | — |
| 반응물 | 5-(5,6-dichloro-1H-indol-2-yl)-2-methoxy-phenylamine | HCID 9836191 | — |
| 생성물 | 3-{3-[5-(5,6-Dichloro-1H-indol-2-yl)-2-methoxy-phenyl]-thioureido}-benzoic acid | HCID 10140976 | — |
반응 단계
3-{3-[5-(5,6-Dichloro-1H-indol-2-yl)-2-methoxy-phenyl]-thioureido}-benzoic acid was prepared from the product of Example 18, Step D, 5-(5,6-dichloro-1H-indol-2-yl)-2-methoxy-phenylamine (0.64 g, 1.72 mmol) and 3-carboxyphenyl isothiocyanate (0.359 g, 2.0 mmol) to give the product as a reddish-tan solid (0.104 g), mp 216-218° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06858739B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-fc2f96c8487d4e54b033454790b8d562 |
| 출처 메모 | uspto-grants-2005_02 |