Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thiophosgene → [5-(1H-indol-2-yl)-2-methoxy-phenyl]-isothiocyanate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thiophosgene | HCID 10040 | — |
| 반응물 | 5-(1H-indol-2-yl)-2-methoxy-phenylamine | HCID 9900204 | — |
| 생성물 | [5-(1H-indol-2-yl)-2-methoxy-phenyl]-isothiocyanate | HCID 22568433 | — |
반응 단계
The product from Example 1, 5-(1H-indol-2-yl)-2-methoxy-phenylamine, (4.76 g, 20 mmol) was reacted with thiophosgene (1.9 mL, 25 mmol) according to the procedure for Example 23, Step A, to give [5-(1H-indol-2-yl)-2-methoxy-phenyl]-isothiocyanate (4.55 g), as a black solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06858739B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-0fec09881fb740ff8ab79f4f7634b1cd |
| 출처 메모 | uspto-grants-2005_02 |