Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Methoxy-2-nitrobenzoic acid → 2-Amino-4-methoxybenzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Methoxy-2-nitrobenzoic acid | HCID 288657 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 2-Amino-4-methoxybenzoic acid | HCID 351010 | 100% |
반응 단계
4-Methoxy-2-nitrobenzoic acid (3 g, 16.4 mmol) was hydrogenated over palladium on carbon (10%, 300 mg) in methanol (80 mL) at room temperature and normal pressure for 18 hours. The reaction mixture was filtered through celite and concentrated to dryness under reduce pressure to give 2.50 g (100%) of the product as a colorless solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07875715B2 |
| 출처 데이터셋 | uspto-grants-2011_01 |
| ORD ID | ord-f8f4666ef20642c2a03ae86bb6637376 |
| 출처 메모 | uspto-grants-2011_01 |