Triethyl orthoacetate → HCID 20183615, 화합물

HRID 255553노트

반응식

HRID 255553 반응식
[NH2:1][C:2]1[CH:3]=[N:4][C:5]2[C:10]([C:11]=1[NH:12][CH2:13][CH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[CH:9][CH:8]=[CH:7][CH:6]=2.[C:21](OCC)(OCC)(OCC)[CH3:22]>C(O)(=O)C>[CH3:21][C:22]1[N:12]([CH2:13][CH2:14][C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)[C:11]2[C:10]3[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=3[N:4]=[CH:3][C:2]=2[N:1]=1

참가 물질

4

반응물 2

HCID 66221Triethyl orthoacetateHCID 20183591HCID 20183591, 화합물

생성물 1

HCID 20183615HCID 20183615, 화합물

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

Using the method of Example 49, 3-amino-4-[2-(phenyl)ethylamino]quinoline (from Example 130, Part B) was reacted with triethyl orthoacetate and acetic acid to provide 2-methyl-1-[2-(phenyl)ethyl]-1H-imidazo[4,5-c]-quinoline.

출처 및 근거

ORD 기록
ord-01a88bb5d74f4f2f84e82c925e37f3b6
출처 데이터셋
uspto-grants-1987_10
특허 번호
US04698348

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