Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dodecane, 1-isocyanato- → N-Octadecyl-N-(D-glucopyranosyl)-N'-dodecylurea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dodecane, 1-isocyanato- | HCID 77873 | — |
| 반응물 | N-octadecylglucopyranosylamine | HCID 13361749 | — |
| 용매 | Ethanol | HCID 702 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | N-Octadecyl-N-(D-glucopyranosyl)-N'-dodecylurea | HCID 13517874 | — |
반응 단계
9 g of the compound from Example 1 are suspended in 160 ml of tetrahydrofuran and 40 ml of ethanol. 4.3 g of dodecyl isocyanate, dissolved in 20 ml of tetrahydrofuran, are added dropwise to this suspension in the course of 20 minutes. When the reaction has ended, the mixture is evaporated in vacuo and the resulting syrup is purified by column chromatography (mobile phase methylene chloride/methanol, 15:1)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04699899 |
| 출처 데이터셋 | uspto-grants-1987_10 |
| ORD ID | ord-991551d7b76645ff896dda6c416665b0 |
| 출처 메모 | uspto-grants-1987_10 |