참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Potassium Nitrate | HCID 24434 | — |
| 반응물 | N-(3-formylphenyl)acetamide | HCID 256849 | — |
| 용매 | Sulfuric Acid | HCID 1118 | — |
| 생성물 | N-(3-formyl-4-nitrophenyl)acetamide | HCID 13987601 | 48.8% |
반응 단계
A solution of potassium nitrate (6.2 g, 61 mmol) in sulfuric acid (30 mL) was added dropwise to stirred solution of N-(3-formylphenyl)acetamide (10.0 g, 61 mmol) in sulfuric acid (120 mL) maintained at 5° C. After 2 hours, the reaction mixture was poured onto ice water (500 mL) and filtered to give N-(3-formyl-4-nitrophenyl)acetamide (6.2 g, 48%) mp 131°-135° C., used without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04701459 |
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| 출처 데이터셋 | uspto-grants-1987_10 |
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| ORD ID | ord-d972c48809d24f6790d4889bc1c8c1e7 |
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| 출처 메모 | uspto-grants-1987_10 |
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