Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylenetetramine → Ethylene carbonate triethylene tetraamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylenetetramine | HCID 5565 | — |
| 반응물 | Ethylene carbonate | HCID 7303 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Ethylene carbonate triethylene tetraamine | HCID 86740738 | — |
반응 단계
Add 2 g of triethylene tetraamine (with an AV of approximately 1180 mg KOH/g) to 20 ml of toluene in a 250 ml flask fitted with a stirrer, condensor and nitrogen inlet. Add 0.6 g ethylene carbonate to the mixture. Reflux the system for 2.5 hours under N2. Strip the system to yield an ethylene carbonate-triethylene tetraamine adduct having an AV of approximately 670 mg KOH/g.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04702851 |
| 출처 데이터셋 | uspto-grants-1987_10 |
| ORD ID | ord-55c355b73fd1451ea2c21d8fa2cecb05 |
| 출처 메모 | uspto-grants-1987_10 |