Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Iodoaniline → N-(4-iodophenyl)-N-methylethanesulphonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Iodoaniline | HCID 10893 | — |
| 반응물 | Ethanesulfonyl chloride | HCID 11667 | — |
| 반응물 | N-(4-iodophenyl)methanesulfonamide | HCID 836147 | — |
| 생성물 | N-(4-iodophenyl)-N-methylethanesulphonamide | HCID 19785600 | — |
반응 단계
The product so obtained was used in place of 4-iodoaniline in the procedure described in Example 3 for the preparation of N-(4-iodophenyl) methanesulphonamide and ethanesulphonyl chloride was used in place of methanesulphonyl chloride. Thus was obtained N-(4-iodophenyl)-N-methylethanesulphonamide as an oil. NMR Spectrum 1.45 (3H, t), 3.00 (2H, q), 3.35 (3H, s), 7.15 (2H, m), 7.70 (2H, m).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05258399 |
| 출처 데이터셋 | uspto-grants-1993_11 |
| ORD ID | ord-5611fef512954a2ea8368584f719a99e |
| 출처 메모 | uspto-grants-1993_11 |