Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cyclohexanone → Prop-2-enenitrile--ethenylbenzene (1/1)
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cyclohexanone | HCID 7967 | — |
| 반응물 | Isoquinoline | HCID 8405 | — |
| 촉매 | Copper(1+) iodide; Copper(I) iodide; Cuprous iodide; Cuprous iodide (CuI) | HCID 24350 | — |
| 용매 | N-methyl-2-pyrrolidone | HCID 13387 | — |
| 생성물 | Prop-2-enenitrile--ethenylbenzene (1/1) | HCID 62696 | 10% |
반응 단계
A solution of 2.0 g. CuI, 1.4 g. isoquinoline (1:1 ratio), 50.0 g. N-methylpyrrolidone solvent, 46.6 g. cyclohexanone and 0.20 g. Lustran SAN 31-1,000 (10% on CuI) was prepared. The resulting coating solution was coated on 7 mil raw PET with number 10 Meyer rod and dried three minutes at 240° F. The coating had very good uniformity and clarity and was gold and blue iridescent and lustrous. The resistivity measured 13-20×107 Ω/sq. The solution after time showed some precipitation, which crystals were redissolved upon reheating.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05259992 |
| 출처 데이터셋 | uspto-grants-1993_11 |
| ORD ID | ord-3110b0bfc3814e4280160de68cfb5d7b |
| 출처 메모 | uspto-grants-1993_11 |