Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl Ether → 5-Norbornene-2-carboxylic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | Acrylic Acid | HCID 6581 | — |
| 반응물 | Cyclopentadiene | HCID 7612 | — |
| 생성물 | 5-Norbornene-2-carboxylic acid | HCID 78949 | 82% |
반응 단계
49.5 g of acrylic acid was added to 49.9 g of cyclopentadiene and 40 ml of diethyl ether, and a reaction was allowed to react at room temperature for 2 hr with stirring. After the completion of the reaction, the reaction mixture was concentrated and purified by distillation to give 78.0 g (yield: 82%) of an intended product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05260257 |
| 출처 데이터셋 | uspto-grants-1993_11 |
| ORD ID | ord-27035d7ebe8f4b13943e774c599ac188 |
| 출처 메모 | uspto-grants-1993_11 |