Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → 3-(3-(2-(2-Butoxyethoxy) ethoxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | 3-(3-(2-(2-Butoxyethoxy)ethoxy)-1,2,5-thiadiazol-4-yl)pyridine | HCID 19075324 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 3-(3-(2-(2-Butoxyethoxy) ethoxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide | HCID 19075254 | — |
반응 단계
A mixture of methyl iodide (0.5 ml, 9 mmol) and 3-(4-(2-(2-butoxyethoxy) ethoxy)-1,2,5-thiadiazol-3-yl)pyridine (3 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05260311 |
| 출처 데이터셋 | uspto-grants-1993_11 |
| ORD ID | ord-a72b0d0968184ca7b2071e3466cafd2c |
| 출처 메모 | uspto-grants-1993_11 |