Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-(4-methoxyphenyl)-N-methylmethanamine → 4-(N-(4-methoxybenzyl)-N-methylamino)-1-(4-nitrophenyl)piperidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-(4-methoxyphenyl)-N-methylmethanamine | HCID 485407 | — |
| 반응물 | 1-(4-Nitrophenyl)piperidin-4-one | HCID 3842562 | — |
| 생성물 | 4-(N-(4-methoxybenzyl)-N-methylamino)-1-(4-nitrophenyl)piperidine | HCID 19784354 | 72.4% |
반응 단계
3.0 g (13.6 mmol) of 1-(4-nitrophenyl)-4-piperidone and 2.0 g (13.6 mmol) of N-(4-methoxybenzyl)-N-methylamine were reacted in a similar manner to Example 1. 3.5 g of 4-(N-(4-methoxybenzyl)-N-methylamino)-1-(4-nitrophenyl)piperidine were obtained. Melting point 144°-145° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05260318 |
| 출처 데이터셋 | uspto-grants-1993_11 |
| ORD ID | ord-7f9b91675af14320a1c9c71b9336bdf2 |
| 출처 메모 | uspto-grants-1993_11 |