2-Naphthoyl chloride → HCID 10083909, 화합물
반응식
[CH3:1][NH:2][C:3](=[S:6])[NH:4][NH2:5].[CH:7]1[C:16]2[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=2)[CH:10]=[CH:9][C:8]=1[C:17](Cl)=[O:18]>N1C=CC=CC=1>[CH3:1][NH:2][C:3](=[S:6])[NH:4][NH:5][C:17]([C:8]1[CH:9]=[CH:10][C:11]2[C:16](=[CH:15][CH:14]=[CH:13][CH:12]=2)[CH:7]=1)=[O:18]참가 물질
4
실험 절차
To a stirred room temperature solution of 4-methyl-thiosemicarbazide (5.91 g, 5.62×10-2 mole) and pyridine (150 ml) was added 2-naphthoyl chloride (10.7 g, 5.61×10-2 mole). After stirring overnight, the pyridine was evaporated at reduced pressure. The concentrate was treated with water and the undissolved product was collected by filtration and dried by suction. Crystallization from acetone/ethanol afforded off-white needles, Mp 211° C. (decomp).
후처리
- customthe pyridine was evaporated at reduced pressure
- additionThe concentrate was treated with water
- filtrationthe undissolved product was collected by filtration
- customdried by suction
- customCrystallization from acetone/ethanol afforded off-white needles, Mp 211° C. (decomp)
출처 및 근거
- ORD 기록
- ord-0a7966e8e07f45e78d515898886e0cf5
- 출처 데이터셋
- uspto-grants-1993_11
- 특허 번호
- US05260450
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