참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | Barium(2+) dichloride | HCID 5360350 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Sulfuric Acid | HCID 1118 | — |
| 생성물 | Barium Sulfate | HCID 24414 | — |
| 생성물 | Barium(2+) dichloride | HCID 5360350 | — |
반응 단계
Aqueous solutions of barium chloride (0.008 mol/1) and sulfuric acid (0.005 mol/1) were prepared by dissolving 1.974 gm of barium chloride (special reagent grade) and 0.505 gm of sulfuric acid (special reagent grade) into 1,000 gm of ion-exchanged water. Each solution was heated at 70° C. The barium chloride solution was added dropwise over a period of 10 minutes to the sulfuric acid solution, while the latter was stirred at 1,000 rpm by a U-shaped blade. After the addition, the mixture was stirred for a further 3 minutes to complete the reaction. The mixture was kept at pH 3.5 during the reaction. After cooling to the room temperature, the reaction mixture was filtered through a 5C filter paper, washed with water, and dried at 105° C. for 2 hours to obtain 1.12 gm of barium sulfate powder.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US05262148 |
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| 출처 데이터셋 | uspto-grants-1993_11 |
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| ORD ID | ord-aeade34999b442e3b364c7d8ea9abb78 |
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| 출처 메모 | uspto-grants-1993_11 |
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