4-Ethylpyridine → 1-(4-Methylphenyl)-3-(4-pyridyl)-butane

HRID 257463

반응식

HRID 257463 반응식
[CH2:1]([C:3]1[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=1)[CH3:2].[CH3:9][C:10]1[CH:18]=[CH:17][C:13]([CH2:14][CH2:15]Br)=[CH:12][CH:11]=1>>[CH3:9][C:10]1[CH:18]=[CH:17][C:13]([CH2:14][CH2:15][CH:1]([C:3]2[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=2)[CH3:2])=[CH:12][CH:11]=1

참가 물질

3

반응물 2

HCID 108224-EthylpyridineHCID 5706804-Methylphenethyl bromide

생성물 1

HCID 197833041-(4-Methylphenyl)-3-(4-pyridyl)-butane수율 98.4%

실험 절차

1.0 g (9.35 mmol) of 4-ethylpyridine and 1.86 g (9.35 mmol) of 4-methylphenethyl bromide were reacted in the same manner as in Example 1. The reaction product was purified to obtain 2.07 g of the desired compound (yield: 98.4%). The resulting compound was identified as 1-(4-methylphenyl)-3-(4-pyridyl)-butane (hereinafter referred to as compound 7) by the following analytical results.

후처리

  1. customThe reaction product was purified

출처 및 근거

ORD 기록
ord-b94f3e175a914bafa6eb4e78d47d9684
출처 데이터셋
uspto-grants-1993_11
특허 번호
US05262420

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