Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Ethylpyridine → 1-(2,6-Dichlorophenyl)-3-(4-pyridyl)butane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Ethylpyridine | HCID 10822 | — |
| 반응물 | 2-(2-Bromoethyl)-1,3-dichlorobenzene | HCID 13480195 | — |
| 생성물 | 1-(2,6-Dichlorophenyl)-3-(4-pyridyl)butane | HCID 19783313 | 55.3% |
반응 단계
1.0 g (9.35 mmol) of 4-ethylpyridine and 2.37 g (9.35 mmol) of 2,6-dichlorophenethyl bromide were reacted in the same manner as in Example 1. The reaction product was purified to obtain 1.45 g of the desired compound (yield: 55.3%). The resulting compound was identified as 1-(2,6-dichlorophenyl)-3-(4-pyridyl)-butane (hereinafter referred to as compound 11) by the following analytical results.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05262420 |
| 출처 데이터셋 | uspto-grants-1993_11 |
| ORD ID | ord-ee4c7f6b2d9949818626607b3a34d2d8 |
| 출처 메모 | uspto-grants-1993_11 |