3-Ethyl-4-methylpyridine → 1-(3-Chlorophenyl)-3-(3-ethyl-4-pyridyl)-propane

HRID 257472

반응식

HRID 257472 반응식
[CH2:1]([C:3]1[CH:4]=[N:5][CH:6]=[CH:7][C:8]=1[CH3:9])[CH3:2].[Cl:10][C:11]1[CH:12]=[C:13]([CH:17]=[CH:18][CH:19]=1)[CH2:14][CH2:15]Br>>[Cl:10][C:11]1[CH:12]=[C:13]([CH2:14][CH2:15][CH2:9][C:8]2[CH:7]=[CH:6][N:5]=[CH:4][C:3]=2[CH2:1][CH3:2])[CH:17]=[CH:18][CH:19]=1

참가 물질

3

반응물 2

HCID 682543-Ethyl-4-methylpyridineHCID 1401401-(2-Bromoethyl)-3-chlorobenzene

생성물 1

HCID 197833501-(3-Chlorophenyl)-3-(3-ethyl-4-pyridyl)-propane수율 50.7%

실험 절차

1.13 g (9.35 mmol) of 3-ethyl-4-methylpyridine and 2.05 g (9.35 mmol) of m-chlorophenethyl bromide were reacted in the same manner as in Example 1. The reaction product was purified to obtain 1.23 g of the desired compound (yield: 50.7%).

후처리

  1. customThe reaction product was purified

출처 및 근거

ORD 기록
ord-e82411eb88074f858b4cae795b5ce223
출처 데이터셋
uspto-grants-1993_11
특허 번호
US05262420

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