Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Iodoethane → 1-Phenyl-3-(3-n-propyl-4-pyridyl)butane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Iodoethane | HCID 6340 | — |
| 반응물 | 1-Phenyl-3-(3-methyl-4-pyridyl)butane | HCID 19783297 | — |
| 반응물 | Lithium diisopropylamine | HCID 45051747 | — |
| 생성물 | 1-Phenyl-3-(3-n-propyl-4-pyridyl)butane | HCID 19783320 | 15.6% |
반응 단계
2.1 g (9.35 mmol) of 1-phenyl-3-(3-methyl-4-pyridyl)butane, 1.46 g (9.35 mmol) of ethyl iodide and 2 equivalent of lithium-diisopropylamine were reacted in the same manner as in Example 1. The reaction product was purified to obtain 0.37 g of the desired compound (yield: 15.6%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05262420 |
| 출처 데이터셋 | uspto-grants-1993_11 |
| ORD ID | ord-050c0500979a4433a4718a4be18e859c |
| 출처 메모 | uspto-grants-1993_11 |