Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl acetone → (E)-1-(3-ethyl-4-pyridyl)-2-methyl-4-phenyl-1-butene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl acetone | HCID 17355 | — |
| 반응물 | 3-Ethyl-4-methylpyridine | HCID 68254 | — |
| 생성물 | (E)-1-(3-ethyl-4-pyridyl)-2-methyl-4-phenyl-1-butene | HCID 14883803 | 69.5% |
반응 단계
The procedure of Example 41 was repeated with the exception that 3.5 g of benzyl acetone in place of cinnamic aldehyde and 2.26 g of 3-ethyl-4-methylpyridine were used in Example 41, to obtain 3.26 g (yield: 59.8%) of (E)-1-(3-ethyl-4-pyridyl)-2-methyl-4-phenyl -1-butene (hereinafter referred to as compound 55) and o.95 g (yield: 17.4%) of (Z)-1-(3-ethyl-4-pyridyl)-2-methyl-4-phenyl-1-butene (hereinafter referred to as compound 56). The analytical results are shown below.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05262420 |
| 출처 데이터셋 | uspto-grants-1993_11 |
| ORD ID | ord-8b990d7f82d54f9b834fc6ef6159ea3e |
| 출처 메모 | uspto-grants-1993_11 |