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HRID 257491생성일: 2026년 10월 26일

Benzyl acetone → (E)-1-(3-ethyl-4-pyridyl)-2-methyl-4-phenyl-1-butene

https://huagongshe.com/reaction/257491

반응식

참여 물질

역할이름HCID투입량
반응물Benzyl acetoneHCID 17355—
반응물3-Ethyl-4-methylpyridineHCID 68254—
생성물(E)-1-(3-ethyl-4-pyridyl)-2-methyl-4-phenyl-1-buteneHCID 1488380369.5%

반응 단계

The procedure of Example 41 was repeated with the exception that 3.5 g of benzyl acetone in place of cinnamic aldehyde and 2.26 g of 3-ethyl-4-methylpyridine were used in Example 41, to obtain 3.26 g (yield: 59.8%) of (E)-1-(3-ethyl-4-pyridyl)-2-methyl-4-phenyl -1-butene (hereinafter referred to as compound 55) and o.95 g (yield: 17.4%) of (Z)-1-(3-ethyl-4-pyridyl)-2-methyl-4-phenyl-1-butene (hereinafter referred to as compound 56). The analytical results are shown below.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05262420
출처 데이터셋uspto-grants-1993_11
ORD IDord-8b990d7f82d54f9b834fc6ef6159ea3e
출처 메모uspto-grants-1993_11