Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyldioxirane → 1-Hydroxy-2,6-diphenyl-3-methylpiperidin-4-yl Laurate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyldioxirane | HCID 115197 | — |
| 반응물 | 2,6-Diphenyl-3-methylpiperidin-4-yl Laurate | HCID 54052528 | — |
| 생성물 | 1-Hydroxy-2,6-diphenyl-3-methylpiperidin-4-yl Laurate | HCID 54551106 | 99.4% |
반응 단계
The general procedure of Example 2 is repeated using 11.5 g (25.5 mmol) of 2,6-diphenyl-3-methylpiperidin-4-yl laurate and 570 mL (25.5 mmol) of dimethyldioxirane (0.045M in acetone). 11.8 g (99% yield) of the title compound is isolated: mp 84°-91° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05262538 |
| 출처 데이터셋 | uspto-grants-1993_11 |
| ORD ID | ord-bd28bc9a3f394ae3a460136e6323746f |
| 출처 메모 | uspto-grants-1993_11 |