Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Allyl Mercaptan → 4-Allylsulfanylmethyl-2,2-dimethyl-6-thiophen-3-yl-1,2-dihydroquinoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Allyl Mercaptan | HCID 13367 | — |
| 반응물 | N-bromobutanimide | HCID 67184 | — |
| 반응물 | 2,2,4-Trimethyl-6-thiophen-3-yl-1,2-dihydroquinoline | HCID 22566532 | — |
| 생성물 | 4-Allylsulfanylmethyl-2,2-dimethyl-6-thiophen-3-yl-1,2-dihydroquinoline | HCID 22566534 | — |
반응 단계
2,2,4-Trimethyl-6-thiophen-3-yl-1,2-dihydroquinoline was brominated with NBS using the procedure described in Example 1 and then coupled with allyl mercaptan using the procedure described in Example 2 to provide 22 mg of the title compound as a oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06858627B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-2ae737324b1e4979a5f2376838cc0e72 |
| 출처 메모 | uspto-grants-2005_02 |