참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | 2-Thiopheneacetic acid | HCID 15970 | — |
| 반응물 | Ethyl 2-methylidenebutanoate | HCID 291416 | — |
| 생성물 | Ethyl 2-(acetylthiomethyl)butanoate | HCID 15025921 | — |
반응 단계
Ethyl 2-ethylpropenoate (5 g, 39 mmol) was diluted with 5.6 mL (78 mmol) of thiolacetic acid and stirred at 65° C. for 36 h. The mixture was then diluted with ether, washed with water and the organic phase was dried with Na2SO4. Evaporation to dryness yielded the title material as an orange oil which was used as such for the next step.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05266568 |
|---|
| 출처 데이터셋 | uspto-grants-1993_11 |
|---|
| ORD ID | ord-ddda9115889046ae9570164ebc99bd6f |
|---|
| 출처 메모 | uspto-grants-1993_11 |
|---|
