Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Iodide → HCID 178502576, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Iodide | HCID 5238 | — |
| 반응물 | Phosphinecarboxylic acid, 1,1-diethoxy-, methyl ester, 1-oxide | HCID 170573 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | HCID 178502576 | HCID 178502576 | — |
반응 단계
A solution of 5.9 parts of diethyl methoxycarbonylphosphonate and 4.5 parts of sodium iodide was stirred at room temperature in 50 parts of tetrahydrofuran for 60 hours. The resulting mixture was filtered to give 3.5 parts of the desired ethyl sodium methoxycarbonylphosphonate, m.p. 123° d.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04033749 |
| 출처 데이터셋 | uspto-grants-1977_07 |
| ORD ID | ord-7f8fb2dabf104e6b91e11cc6e135581c |
| 출처 메모 | uspto-grants-1977_07 |