Sodium Iodide → HCID 178502576, 화합물

HRID 258489

반응식

HRID 258489 반응식
[CH3:1][O:2][C:3]([P:5](=[O:12])([O:9][CH2:10][CH3:11])[O:6]CC)=[O:4].[I-].[Na+:14]>O1CCCC1>[CH3:1][O:2][C:3]([P:5](=[O:6])([OH:12])[OH:9])=[O:4].[CH2:10]([Na:14])[CH3:11]

참가 물질

4

반응물 2

HCID 5238Sodium IodideHCID 170573Phosphinecarboxylic acid, 1,1-diethoxy-, methyl ester, 1-oxide

생성물 1

HCID 178502576HCID 178502576, 화합물

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

A solution of 5.9 parts of diethyl methoxycarbonylphosphonate and 4.5 parts of sodium iodide was stirred at room temperature in 50 parts of tetrahydrofuran for 60 hours. The resulting mixture was filtered to give 3.5 parts of the desired ethyl sodium methoxycarbonylphosphonate, m.p. 123° d.

후처리

  1. filtrationThe resulting mixture was filtered

출처 및 근거

ORD 기록
ord-7f8fb2dabf104e6b91e11cc6e135581c
출처 데이터셋
uspto-grants-1977_07
특허 번호
US04033749

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