Formaldehyde → Formaldehyde melamine silicate

HRID 258530

반응식

HRID 258530 반응식
[Si:1]([OH:5])([OH:4])([OH:3])[OH:2].[N:6]1[C:13]([NH2:14])=[N:12][C:10]([NH2:11])=[N:9][C:7]=1[NH2:8].[CH2:15]=[O:16].S(=O)(=O)(O)O>>[Si:1]([OH:5])([OH:4])([OH:3])[OH:2].[N:6]1[C:13]([NH2:14])=[N:12][C:10]([NH2:11])=[N:9][C:7]=1[NH2:8].[CH2:15]=[O:16]

참가 물질

4

반응물 3

HCID 712FormaldehydeHCID 1118Sulfuric AcidHCID 69385141Melamine silicate

생성물 1

HCID 131710831Formaldehyde melamine silicate

실험 절차

The said melamine silicate as produced in Example VII is added to about 2 mols of formaldehyde in an aqueous solution and dilute sulfuric acid is added until the pH is 4 to 5.5, then heated to 70° to 100° , while agitating, for 15 to 60 minutes, thereby producing a white, solid resin, poly (formaldehyde melamine silicate). The said resin is not soluble in acetic acid and is resistent to strong acids and alkalis. On heating, the said resin softens very little and is destroyed before it will melt.

후처리

  1. additionis added until the pH is 4 to 5.5
  2. temperatureheated to 70° to 100°

출처 및 근거

ORD 기록
ord-32daf0e4646d47c6af7b5c1bd78bd847
출처 데이터셋
uspto-grants-1977_07
특허 번호
US04033935

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