Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 6-Chloro-2-nitrophenoxyacetic acid ethyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Ethyl chloroacetate | HCID 7751 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Phenol, 2-chloro-6-nitro- | HCID 11784 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 6-Chloro-2-nitrophenoxyacetic acid ethyl ester | HCID 54160692 | — |
반응 단계
A solution of 6-chloro-2-nitrophenol (1.7 g.) and ethyl chloroacetate (2.1 ml.) in dimethylformamide (12 ml.) with potassium carbonate (1.5 g.) was stirred at 75°-80° C. for 3 hours. The mixture as poured into water (120 ml.) and extracted with ethyl acetate (4× 50 ml.). The organic layer on evaporation yielded 6-chloro-2-nitrophenoxyacetic acid ethyl ester as a yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04033951 |
| 출처 데이터셋 | uspto-grants-1977_07 |
| ORD ID | ord-a64d4780c9144246800a729ca3dd90ae |
| 출처 메모 | uspto-grants-1977_07 |