HCID 12841761, 화합물 → 3-beta-(4-Carbamoylmethoxyphenylacetamido)ethylamino-1-(2-cyanophenoxy)-2-propanol

HRID 258755노트

반응식

HRID 258755 반응식
[NH2:1][CH2:2][CH2:3][NH:4][CH2:5][CH:6]([OH:17])[CH2:7][O:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[C:15]#[N:16].[C:18]([CH2:21][O:22][C:23]1[CH:28]=[CH:27][C:26]([CH2:29][C:30](OCC)=[O:31])=[CH:25][CH:24]=1)(=[O:20])[NH2:19]>>[C:18]([CH2:21][O:22][C:23]1[CH:28]=[CH:27][C:26]([CH2:29][C:30]([NH:1][CH2:2][CH2:3][NH:4][CH2:5][CH:6]([OH:17])[CH2:7][O:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[C:15]#[N:16])=[O:31])=[CH:25][CH:24]=1)(=[O:20])[NH2:19]

참가 물질

3

반응물 2

HCID 12841761HCID 12841761, 화합물HCID 20499321HCID 20499321, 화합물

생성물 1

HCID 543263233-beta-(4-Carbamoylmethoxyphenylacetamido)ethylamino-1-(2-cyanophenoxy)-2-propanol

실험 절차

In a similar manner using 2.36 g. of 3-(β-aminoethylamino)-1-(2-cyanophenoxy)-2-propanol and 2.37 g. of ethyl 4-carbamoylmethoxyphenylacetate as starting materials there is obtained 3-β-(4-carbamoylmethoxyphenylacetamido)ethylamino-1-(2-cyanophenoxy)-2-propanol, isolated as its hydrogen oxalate, m.p. 123°-125° C. after crystallisation from ethyl acetate.

출처 및 근거

ORD 기록
ord-a9327a5df53b438999d1a72721e5e397
출처 데이터셋
uspto-grants-1977_07
특허 번호
US04034106

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