참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Diethyl Carbonate | HCID 7766 | — |
| 반응물 | HCID 178418320 | HCID 178418320 | — |
| 반응물 | HCID 178418384 | HCID 178418384 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | Di-n-decyl-n-tetradecylcarbinol | HCID 19690406 | — |
반응 단계
Decylmagnesium bromide (0.66 mole) in ethyl ether is slowly added to 0.33 moles of diethylcarbonate in 100 ml ethyl ether and stirred for one hour at 30° C. (nitrogen atmosphere). Tetradecylmagnesium bromide (0.33 moles) is slowly added to the solution and stirred for one hour at 30° C. The mixture is then slowly poured into 600 ml of a cold 10% HCl solution. The organic layer is dried with magnesium sulfate and the ethyl ether evaporated off to give di-n-decyl-n-tetradecylcarbinol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05728907 |
|---|
| 출처 데이터셋 | uspto-grants-1998_03 |
|---|
| ORD ID | ord-108d826840d345cdb28e811cd9a5ff6a |
|---|
| 출처 메모 | uspto-grants-1998_03 |
|---|
