Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Carbonate → 2-[3-Bis(2-hydroxyethyl)aminopropyl]amino-quinoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | 2-Chloroquinoline | HCID 11928 | — |
| 반응물 | (3-Aminopropyl)diethanolamine | HCID 21088 | — |
| 용매 | Isopropanol | HCID 3776 | — |
| 생성물 | 2-[3-Bis(2-hydroxyethyl)aminopropyl]amino-quinoline | HCID 21424676 | — |
반응 단계
A mixture of 5.05 g. of 2-chloroquinoline, 5.5 g. of bis(2-hydroxyethyl)aminopropylamine and 3.0 g. of sodium carbonate is heated in 20 ml. of refluxing isopropanol for 24 hours. The reaction mixture is then filtered, solvent removed in vacuo and the residue chromatographed over silica gel to obtain an oil of 2-[3-bis(2-hydroxyethyl)aminopropyl]amino-quinoline.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04035367 |
| 출처 데이터셋 | uspto-grants-1977_07 |
| ORD ID | ord-03178fbcc19d4bcd8274cb500c301743 |
| 출처 메모 | uspto-grants-1977_07 |