Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isopropanol → HCID 21424687, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isopropanol | HCID 3776 | — |
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | (3-Aminopropyl)diethanolamine | HCID 21088 | — |
| 반응물 | 4-Chloroquinoline | HCID 69140 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | HCID 21424687 | HCID 21424687 | — |
반응 단계
A mixture of 5.0 g. of 4-chloroquinoline, 7.2 g. of bis(2-hydroxyethyl)aminopropylamine, 3.0 g. of sodium carbonate and 25 ml. of isopropanol is heated in a pressure vessel at 150° C. for 17 hours. The resulting mixture is diluted with chloroform, filtered and purified by filtering over silica gel to obtain an oil of 4-[3-bis(2-hydroxyethyl)aminopropyl]amino-quinoline.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04035367 |
| 출처 데이터셋 | uspto-grants-1977_07 |
| ORD ID | ord-ffe936cf2a1e425e9c83948efb67bf2b |
| 출처 메모 | uspto-grants-1977_07 |