Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Di-n-decyl-n-tetradecylmethylchloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Calcium Chloride | HCID 5284359 | — |
| 반응물 | Di-n-decyl-n-tetradecylcarbinol | HCID 19690406 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Di-n-decyl-n-tetradecylmethylchloride | HCID 19690403 | — |
반응 단계
One mole of di-n-decyl-n-tetradecylcarbinol is added to 0.2 liters of methylene chloride and 0.32 moles calcium chloride. Approximately 1.5 moles of HCl gas is slowly bubbled through the solution. The product mixture is then washed with 1 liter of a 10% sodium carbonate solution. The organic layer is dried with magnesium sulfate and the methylene chloride is evaporated off to give di-n-decyl-n-tetradecyl-methylchloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05728907 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-3272ce8059be4591a93fe2fa3200dcab |
| 출처 메모 | uspto-grants-1998_03 |