Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Suprofen → p-(2-Thenoyl)hydratropoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Suprofen | HCID 5359 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | p-(2-Thenoyl)hydratropoyl chloride | HCID 11747905 | — |
반응 단계
A mixture of 5.2 parts of p-(2-thenoyl)hydratropic acid, 4.8 parts of thionyl chloride and 32 parts of anhydrous benzene is stirred and refluxed for 3h. 30. The reaction mixture is evaporated and the residue is evaporated once more from benzene, yielding p-(2-thenoyl)hydratropoyl chloride as a residue.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04035376 |
| 출처 데이터셋 | uspto-grants-1977_07 |
| ORD ID | ord-6b9439048f53451e9dbe69fab35877a6 |
| 출처 메모 | uspto-grants-1977_07 |