Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N,N-Dimethylbenzylamine → HCID 21425139, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N,N-Dimethylbenzylamine | HCID 7681 | — |
| 반응물 | Trichloropentylsilane | HCID 7885 | — |
| 반응물 | alpha-Bromoethyltriethoxysilane | HCID 21425138 | — |
| 용매 | Methyl Ethyl Ketone | HCID 6569 | — |
| 생성물 | HCID 21425139 | HCID 21425139 | — |
반응 단계
In a manner like that used for the preparation of alpha-bromoethyltriethoxysilane, alpha-bromoamyltriethoxysilane is prepared in two steps from amyltrichlorosilane (commercially available). One-quarter mole of alpha-bromoamyltriethoxysilane (78.5g) is refluxed for 12 hours with 0.25 moles (33.75g) of benzyldimethylamine in 125 ml. of 2-butanone. The product, alpha-(benzyldimethylammonio)ethyltriethoxysilane bromide is isolated by removing the solvent under vacuum.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04035411 |
| 출처 데이터셋 | uspto-grants-1977_07 |
| ORD ID | ord-c4e838e1b7d3491287275096ae3d8e91 |
| 출처 메모 | uspto-grants-1977_07 |