Acrylamide → Acrylamide 2-Methacryloyloxyethyl Trimethyl Ammonium

반응식

[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[C:6]([O:11][CH2:12][CH2:13][N+:14]([CH3:17])([CH3:16])[CH3:15])(=[O:10])[C:7]([CH3:9])=[CH2:8]>>[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[C:6]([O:11][CH2:12][CH2:13][N+:14]([CH3:17])([CH3:15])[CH3:16])(=[O:10])[C:7]([CH3:9])=[CH2:8]

참가 물질

반응물 2

HCID 6579Acrylamide

HCID 78739Methacrylylcholine

생성물 1

HCID 86735511Acrylamide 2-Methacryloyloxyethyl Trimethyl Ammonium

실험 절차

Acrylamide (AM) (49.6 g.), 2-methacryloyloxyethyl trimethyl ammonium methosulfate (METAMS) (26.0 g. of a 40% aqueous solution), distilled water (44.4 g.), Tween 85 (30.0 g.), and Mentor 28 (50.0 g.) were combined and reacted according to the procedure of Example 31. The pH of the emulsion was adjusted to 6.0; the maximum temperature reached was 71° C.; the product was a stable emulsion.

후처리

distillationof a 40% aqueous solution), distilled water (44.4 g.), Tween 85 (30.0 g.), and Mentor 28 (50.0 g.)
customreacted
customreached was 71° C.

출처 및 근거

ORD 기록: ord-a234627dec74419db08ec114ddbb8683
출처 데이터셋: uspto-grants-1979_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04147681

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