참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-Ethylhexylamine | HCID 7719 | — |
| 반응물 | Ethyl cyanoacetate | HCID 7764 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-cyano-N-(2-ethylhexyl)acetamide | HCID 4590704 | — |
반응 단계
To ethylcyanoacetate (141 g., 1.25 mole) is slowly added 2-ethylhexylamine (129 g., 1.0 mole) over a period of 0.5 hours. The solution is then gradually heated to 154° C. and the ethanol formed is collected over a period of 1.75 hours. The solution is then stripped of all volatiles boiling at or below 88° C./3.0 mm to give N-(2-ethylhexyl)cyanoacetamide, 201.5 g.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04038065 |
|---|
| 출처 데이터셋 | uspto-grants-1977_07 |
|---|
| ORD ID | ord-f98c1453371a44e88d48735337fef260 |
|---|
| 출처 메모 | uspto-grants-1977_07 |
|---|
