Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → L-Lysine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | L-Lysine monohydrochloride | HCID 69568 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | L-Lysine | HCID 5962 | 97.6% |
반응 단계
Into the reaction apparatus used in Example 1, 160 g of ethyl alcohol, 18.3 g of lysine hydrochloride and 4.0 g of sodium hydroxide were charged. The resulting mixture was heated, refluxing the solvent, while being stirred, and was kept for 3 hours. The resultant product was cooled to room temperature and the by-product sodium chloride was filtered off therefrom. The solvent was distilled off from the obtained product to obtain 14.3 g of lysine in a syrup state. The lysine obtained, 15.8 g of allantoin and 150 ml of water were charged into the apparatus.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04038287 |
| 출처 데이터셋 | uspto-grants-1977_07 |
| ORD ID | ord-26ef38e707344f00b1bbdc6e88b1c41d |
| 출처 메모 | uspto-grants-1977_07 |