Butyric Acid → Heptafluorobutyric acid

HRID 259473

반응식

HRID 259473 반응식
[F:1][C:2]([F:13])([C:9]([F:12])([F:11])[F:10])[C:3]([F:8])([F:7])[C:4]([F:6])=[O:5].C(O)(=[O:18])CCC.C(OC(=O)CCC)(=O)CCC>>[F:10][C:9]([F:12])([F:11])[C:2]([F:13])([F:1])[C:3]([F:8])([F:7])[C:4]([OH:18])=[O:5].[C:4]([F:6])(=[O:5])[CH2:3][CH2:2][CH3:9]

참가 물질

5

반응물 3

HCID 264Butyric AcidHCID 7798Butyric anhydrideHCID 67632Heptafluorobutyroyl fluoride

생성물 2

HCID 9777Heptafluorobutyric acidHCID 68035Butanoyl fluoride

실험 절차

The following run illustrates the metathetical reaction of impure heptafluorobutyryl fluoride with butyric acid in the presence of butyric anhydride to give heptafluorobutyric acid and butyryl fluoride and the recovery of products from the reaction mixture by fractional distillation.

출처 및 근거

ORD 기록
ord-f0fd27ea775447efb4ba9fb622217ab9
출처 데이터셋
uspto-grants-1977_07
특허 번호
US04038310

연결된 노트

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