Benzyl chloride hydrochloride → 5-Benzyloxycarbonyl-6-benzyl-4,5,6,7-tetrahydro-thieno[2,3-c]pyridine
반응식
[C:1]([CH:4]1[NH:9][CH2:8][C:7]2[S:10][CH:11]=[CH:12][C:6]=2[CH2:5]1)([OH:3])=[O:2].Cl.[CH2:14](Cl)[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>C(O)(C)C>[CH2:14]([O:2][C:1]([CH:4]1[N:9]([CH2:14][C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)[CH2:8][C:7]2[S:10][CH:11]=[CH:12][C:6]=2[CH2:5]1)=[O:3])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1참가 물질
4
실험 절차
Obtained according to a procedure analogous to that of Example 7, from 5-carboxy-4,5,6,7-tetrahydro-thieno[2,3-c]pyridine (Example 6) and benzyl chloride. Hydrochloride: pale yellow crystals; M.p. 135°-140° C. (isopropanol); Yield: 53%.
후처리
- customObtained
출처 및 근거
- ORD 기록
- ord-b671f540aa9b4a5aa48ac542def02e55
- 출처 데이터셋
- uspto-grants-1979_04
- 특허 번호
- US04147787
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