Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,5-Dihydroxybenzoic acid → Methyl Gentisate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,5-Dihydroxybenzoic acid | HCID 3469 | — |
| 반응물 | Ethyl 5-formyl-2-hydroxybenzoate | HCID 18930679 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Methyl Gentisate | HCID 75077 | 94% |
반응 단계
2,5-Dihydroxybenzoic acid was converted to its methyl ester using catalytic sulfuric acid in methanol following the same protocol as for esterification 2c in 94% yield. mp 86.4°-88.5° C. IR(KBr): cm-1 3346, 1684.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05523302 |
| 출처 데이터셋 | uspto-grants-1996_06 |
| ORD ID | ord-a951e7e6815d485cb58f68faeb832be4 |
| 출처 메모 | uspto-grants-1996_06 |