Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 1-Amino-p-methoxyphenylmethanephosphonous acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | 4-Methoxybenzaldehyde | HCID 31244 | — |
| 반응물 | HCID 178418291 | HCID 178418291 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 생성물 | 1-Amino-p-methoxyphenylmethanephosphonous acid | HCID 86736441 | — |
반응 단계
A mixture of 13.6 parts anisaldehyde and 8.3 parts ammonium hypophosphite in 100 parts xylene was refluxed with water separation. The xylene was cooled, decanted and the residue boiled with ethanol to give a white solid. Filtration gave DL-1-amino-p-methoxyphenylmethanephosphonous acid, melting point 239°-241° (dec.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04147780 |
| 출처 데이터셋 | uspto-grants-1979_04 |
| ORD ID | ord-24e4c99b0b07489a91a8b31e14f959c8 |
| 출처 메모 | uspto-grants-1979_04 |