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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 259869생성일: 2026년 10월 24일

Allyl glycidyl ether → gamma-Glycidoxypropyltriethoxysilane

https://huagongshe.com/ko/reaction/259869

반응식

참여 물질

역할이름HCID투입량
반응물Allyl glycidyl etherHCID 7838—
반응물TriethoxysilaneHCID 13830—
생성물gamma-GlycidoxypropyltriethoxysilaneHCID 10285662.6%

반응 조건

온도150 °C

반응 단계

140 g (0.85 mol) of hydridotriethoxysilane were mixed with 100 g (0.88 mol) of allyl glycidyl ether, and 10 g of this mixture were initially introduced into a reaction vessel at 95° C. under normal pressure with 100 mg (9.5×10-5 mol) of tetrakis(1-phenyl-3-n-hexyl-1-triazenido) platinum complex. The remainder of the above mentioned was added dropwise to the mixture in the course of 80 minutes, the temperature rose to 160° C. When the addition was complete, the reaction mixture was stirred at 150° C. for an additional 30 minutes. After distillation, 3-glycidoxypropyltriethoxysilane was obtained as a colorless, liquid product in a 62.6% yield.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05523436
출처 데이터셋uspto-grants-1996_06
ORD IDord-f8784502a33042ab84b183fb01eab7f1
출처 메모uspto-grants-1996_06