1-Benzhydrylamino-2-methylpropanephosphonous acid → 1-Amino-1-(thien-2-yl)-methanephosphonous acid

반응식

C([NH:14][CH:15]([C:19]1[S:20][CH:21]=[CH:22][CH:23]=1)[P:16]([OH:18])[OH:17])(C1C=CC=CC=1)C1C=CC=CC=1.C(NC(P(O)O)C(C)C)(C1C=CC=CC=1)C1C=CC=CC=1>>[NH2:14][CH:15]([C:19]1[S:20][CH:21]=[CH:22][CH:23]=1)[P:16]([OH:18])[OH:17]

참가 물질

반응물 2

HCID 213258821-Benzhydrylamino-2-methylpropanephosphonous acid

HCID 213258931-Benzhydrylamino-1-(2-thienyl)-methanephosphonous acid

생성물 1

HCID 213259051-Amino-1-(thien-2-yl)-methanephosphonous acid

실험 절차

The procedure described in Example 36B was repeated using DL-1-benzhydrylamino-1-(2-thienyl)-methanephosphonous acid instead of DL-1-benzhydrylamino-2-methylpropanephosphonous acid to give DL-1-amino-1-(thien-2-yl)-methanephosphonous acid, melting point 229°-230°.

출처 및 근거

ORD 기록: ord-f66f1632550f46c3923fe0807bcbda37
출처 데이터셋: uspto-grants-1979_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04147780

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