Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(+-)-Methyl mandelate → Methyl phenylglyoxalate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (+-)-Methyl mandelate | HCID 78066 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Methyl phenylglyoxalate | HCID 84835 | — |
반응 단계
The procedures of Example 1 were repeated except for employing the above-obtained catalyst (8 ml), feeding air and nitrogen at feed rates of 35 ml/min. and 70 ml/min., respectively, and feeding a methyl mandelate solution comprising methanol and methyl mandelate (6:1, by weight) at a feed rate of 17.0 g/hr., to carry out the gaseous catalytic reaction. There was obtained methyl phenylglyoxylate as α-keto acid ester. The results are set forth in Table 5.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05523459 |
| 출처 데이터셋 | uspto-grants-1996_06 |
| ORD ID | ord-16f44b1b14b84e858f643fd6690b3e3a |
| 출처 메모 | uspto-grants-1996_06 |