Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → HCID 22401314, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Ethyl Acetate | HCID 8857 | — |
| 반응물 | 3-amino-N,N-dimethylbenzylamine | HCID 99294 | — |
| 반응물 | P,P-Diphenylphosphinic azide | HCID 199401 | — |
| 반응물 | 1,2-Dihydro-2-methyl-1-oxo-4-phenyl-3-isoquinoline acetic acid | HCID 10402129 | — |
| 생성물 | HCID 22401314 | HCID 22401314 | — |
반응 단계
Using 1,2-dihydro-2-methyl-1-oxo-4-phenyl-3-isoquinoline acetic acid, diphenylphosphoryl azide and 3-(dimethylaminomethyl)aniline, the reaction was carried out by substantially the same procedure as in Method B of Example 1, followed by treatment of the product with hydrogen chloride in ethyl acetate to give the title compound as a white powdery product. NMR (200 MHz,DMSO-d6) ppm: 2.67(3H,s), 2.69(3H,s), 3.64(3H,s), 4.17(4H,m), 6.9-7.2(4H,m), 7.3-7.7(9H,m), 8.32(1H,m), 9.09(1H,bs)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05527811 |
| 출처 데이터셋 | uspto-grants-1996_06 |
| ORD ID | ord-20135b24567f494ca98b81410a796d51 |
| 출처 메모 | uspto-grants-1996_06 |