Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chlorotrimethylsilane → 2-Benzyl-2-trimethylsilyl-1,3-dithiane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chlorotrimethylsilane | HCID 6397 | — |
| 반응물 | 2-Benzyl-1,3-dithiane | HCID 300291 | — |
| 생성물 | 2-Benzyl-2-trimethylsilyl-1,3-dithiane | HCID 10469008 | 75% |
반응 단계
The title compound of this step was prepared in 75% yield, by the procedure described in JACS 89, (1967), 4347 by E. J. Corey, et al., using 2-benzyl-1,3-dithiane and trimethylsilyl chloride. The product was recrystallized from diethyl ether/pentane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05529988 |
| 출처 데이터셋 | uspto-grants-1996_06 |
| ORD ID | ord-157274fec4e5454391c7c93903080036 |
| 출처 메모 | uspto-grants-1996_06 |