Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Homophthalic acid → 3,3-dimethyl-5-oxo-2,3-dihydro-5H-thiazolo[3,2-b]isoquinoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Homophthalic acid | HCID 66643 | — |
| 반응물 | Sodium Acetate | HCID 517045 | — |
| 반응물 | 2-Amino-2-methylpropane-1-thiol | HCID 521040 | — |
| 용매 | 1,2-Dichlorobenzene | HCID 7239 | — |
| 생성물 | 3,3-dimethyl-5-oxo-2,3-dihydro-5H-thiazolo[3,2-b]isoquinoline | HCID 12593065 | — |
반응 단계
By following the same procedure as in Example 49 using a mixture of 240 mg. of 2-carboxymethylbenzoic acid, 300 mg. of 2-amino-2-methylpropanethiol, 164 mg. of sodium acetate, and 5 ml. of o-dichlorobenzene, 120 mg. of 3,3-dimethyl-5-oxo-2,3-dihydro-5H-thiazolo[3,2-b]isoquinoline was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04163844 |
| 출처 데이터셋 | uspto-grants-1979_08 |
| ORD ID | ord-64cfce68ca0c405c91b0742af24d77f8 |
| 출처 메모 | uspto-grants-1979_08 |