Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Nitro-4-(trifluoromethyl)phenol → 2-Amino-4-(trifluoromethyl)phenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Nitro-4-(trifluoromethyl)phenol | HCID 9816 | — |
| 촉매 | Platinum oxide (PtO) | HCID 82844 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-Amino-4-(trifluoromethyl)phenol | HCID 120246 | — |
반응 단계
82.2 g of 6A was dissolved in 300 ml of ethanol. 0.5 g of platinum oxide catalyst was added and the mixture was hydrogenated at 50 psig. Fresh portions of catalyst were added periodically. The reaction mixture was filtered, and the filtrate was concentrated. The residue was crystallized from water to give 2-amino-4-(trifluoromethyl)phenol (6B).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04164576 |
| 출처 데이터셋 | uspto-grants-1979_08 |
| ORD ID | ord-059b6ae66e85466a99b629334c527693 |
| 출처 메모 | uspto-grants-1979_08 |