Water → N-(3-Hexyl)-4-allyl-3-methyl-2,6-dinitroaniline

HRID 261277

반응식

HRID 261277 반응식
[CH2:1]([C:4]1[CH:9]=[C:8]([N+:10]([O-:12])=[O:11])[C:7](Cl)=[C:6]([N+:14]([O-:16])=[O:15])[C:5]=1[CH3:17])[CH:2]=[CH2:3].C1(C)C(C)=CC=CC=1.O.[CH3:27][CH2:28][CH:29]([NH2:33])[CH2:30][CH2:31][CH3:32]>>[CH3:27][CH2:28][CH:29]([NH:33][C:7]1[C:8]([N+:10]([O-:12])=[O:11])=[CH:9][C:4]([CH2:1][CH:2]=[CH2:3])=[C:5]([CH3:17])[C:6]=1[N+:14]([O-:16])=[O:15])[CH2:30][CH2:31][CH3:32]

참가 물질

5

반응물 4

HCID 962WaterHCID 7237O-XyleneHCID 86062Hexan-3-amineHCID 205638414-Allyl-3-methyl-2,6-dinitrochlorobenzene

생성물 1

HCID 54001796N-(3-Hexyl)-4-allyl-3-methyl-2,6-dinitroaniline

실험 절차

One equivalent of 4-allyl-3-methyl-2,6-dinitrochlorobenzene is dissolved in three volumes of xylene containing two equivalents of 3-hexylamine. The mixture is refluxed for 5 hours and then poured into water. The organic phase is washed with 5% hydrochloric acid and then water, dried over calcium sulfate, and removed in vacuo to leave the above-named product.

후처리

  1. temperatureThe mixture is refluxed for 5 hours
  2. washThe organic phase is washed with 5% hydrochloric acid
  3. dry with materialwater, dried over calcium sulfate
  4. customremoved in vacuo
  5. customto leave the above-named product

출처 및 근거

ORD 기록
ord-18c0fd0b21a644d6af639efadef5afec
출처 데이터셋
uspto-grants-1979_08
특허 번호
US04165231

연결된 노트

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